The technological process for niobium tube extrusion production: preparation, power frequency induction heating (600 + 10˚C), glass powder lubrication, secondary power frequency induction heating (1150 + 10˚C), reaming (reduction of area is less than 20.0%), third power frequency induction heating (1200 + 10˚C), small deformation, extrusion(extrusion ratio is not more than 10, and reduction of area is less than 90%) , air cooling, and finally finished the hot extrusion process of niobium tube.
The niobium seamless tube produced by this method ensures sufficient thermal process plasticity. The disadvantage of niobium fluidity is avoided by means of small deformation extrusion. Performance and dimensions meet user requirements.
Niobium and Niobium Alloys Tube Grade and Standard
Category
Country
Grade
Standard
Tube
USA
R04200, R04210, R04251, R04261
ASTM B394
Niobium and Niobium Alloys Tube Chemical Composition (wt%≤)
Element
Niobium R04200
Niobium R04210
Nb-1%Zirconium R04251
Nb-1%Zirconium R04261
C
0.01
0.01
0.01
0.01
N
0.01
0.01
0.01
0.01
O
0.015
0.025
0.015
0.025
H
0.0015
0.0015
0.0015
0.0015
Zr
0.02
0.02
0.8 to 1.2
0.8 to 1.2
Ta
0.1
0.3
0.1
0.5
Fe
0.005
0.01
0.005
0.01
S
0.005
0.005
0.005
0.005
W
0.03
0.05
0.03
0.05
Ni
0.005
0.005
0.005
0.005
Mo
0.010
0.020
0.010
0.050
Hf
0.02
0.02
0.02
0.02
Ti
0.02
0.03
0.02
0.03
B
2ppm
-
2ppm
-
Al
0.002
0.005
0.002
0.005
Be
0.005
-
0.005
-
Cr
0.002
-
0.002
-
C
0.002
-
0.002
-
Niobium and Niobium Alloys Tube Dimension and Tolerance
Outer Diameter (D)/in (mm)
Outer Diameter Tolerance/in (mm)
Inner Diameter Tolerance/in (mm)
Wall Thickness Tolerance/%
0.187 < D < 0.625 (4.7 < D < 15.9)
± 0.004 (0.10)
± 0.004 (0.10)
10
0.625 < D < 1.000 (15.9 < D < 25.4)
± 0.005 (0.13)
± 0.005 (0.13)
10
1.000 < D < 2.000(25.4 < D < 50.8)
± 0.0075 (0.19)
± 0.0075 (0.19)
10
2.000 < D < 3.000(50.8 < D < 76.2)
± 0.010 (0.25)
± 0.010 (0.25)
10
3.000 < D < 4.000(76.2 < D < 101.6)
± 0.0125 (0.32)
± 0.0125 (0.32)
10
The tolerance can be adjusted based on customer's request.